37.

Ribeiro F. A. L., Ferreira M. M. C., “QSAR MODEL OF THE PHOTOTOXICITY OF POLYCYCLIC AROMATIC HYDROCARBONS”. Caxambu, MG, Brazil, 11-16/11/2001: 1º Simpósio Brasileiro em Química Medicinal, QSAR e Modelagem Molecular: Novas Estratégias em Planejamento Racional de Fármacos [1st Brazilian Symposium on Medicinal Chemistry, QSAR and Molecular Modeling: New Approaches in Drug Design]. Poster APM11. Section: 4. Applications of Multivariate QSAR.


phototoxicity

Name
       Fabiana Alves de Lima Ribeiro, Márcia M. C. Ferreira

Institution/Company
      UNICAMP

Country
      Brasil

First Abstract Title
      QSAR MODEL OF THE PHOTOTOXICITY OF POLYCYCLIC AROMATIC HYDROCARBONS

First Abstract
      Ribeiro, F. A. L.; Ferreira, M. M. C.; Laboratório de Quimiometria Teórica e Aplicada, Instituto de Química
      Universidade Estadual de Campinas, Campinas SP 13083-970.

      The rising preoccupation about the discharge of
      polyciclic aromatic hydrocarbons (PAHs) in the environment, has stimulated the investigation of the properties and
      biological activities of these chemicals, because they are well known to be carcinogenic and toxic compounds. PAHs
      are produced by degradation or incomplete combustion of organic materials, like in the burning of wool and coal,
      exhaust of gasoline and diesel combustion engines, the smoking of tobacco, and other combustion processes in
      which the carbon fuel is not completely converted to CO or CO2.(1) Recent research has demonstrated that when
      exposed to UV radiation, some PAHs can become extremely toxic, a phenomenon known as phototoxicity. The UV
      and visible radiation can be sufficiently energetic to modify the chemical structure of some compounds generating
      biologically active species. Upon the sunlight exposure, some PAHs can undergo rapid structural modifications which
      occurs by photooxidation reactions, and the products originated from these modifications might present toxicity. This
      toxicity is due to p-orbital system of PAHs, which strongly absorb sunlight in the UV and visible light.(2) In this study,
      a QSAR model is built with the aim to predict the phototoxicity of some PAHs using the following electronic
      descriptors: HOMO and LUMO energies, and the difference between them, named as GAP. Firstly, the geometry of all
      molecules were optimized and the frontier orbital energies and GAP were calculated by the semi-empirical method
      AM1 using Spartan software. These three electronic variables, selected to construct the model, don't present
      necessarily a linear correlation with the phototoxicity. Gaussian functions were used to linearize these relationships
      allowing the construction of a linear QSAR model. Experimental phototoxicity for Daphnia magna of PAHs, expressed
      as the median adjusted lethal time ALT, was taken from literature for a set of 14 molecules.(3) The model was
      constructed by partial least square method PLS, using autoscaled data and leave-one-out crossvalidation. Pirouette
      2.02 (Infometrix) and MATLAB (MathWorks Inc) software were used. Two latent variables describing 91.1% of total
      variance showed to be significant, producing a model with correlation coefficient r = 0.967 and validation errors smaller
      than 5% (with a few exceptions). Phototoxicity was predicted for a set of 56 molecules in which experimental
      measurements were not performed yet. benzo[h]pentaphene, naphto[2,3-g]chrysene and coronene are predicted
      among the most phototoxic compounds, whereas acenaphtylene and benzo[a]perylene are not predicted to be.

      ACKNOWLEDGEMENTS. The authors would like to thank Lucicleide R. Cirino for her help in making calculations,
      CAPES, FAPESP and FAEP for financial support, and CENAPAD for the computational support. REFERENCES 1 -
      BAIRD, C.; Environmental Chemistry, 2nd ed., W. H. Freeman and Company, USA, 1995. 2 - SCHAEFFER, FAIC, D
      J. & LARSON, R. A., The Chemist, July/August, 1999, 18-24. 3 - MEKENYAN, O. G.; ANKLEY, G. T.; VEITH, G. D.;
      CALL, D. J, Chemosfere, v. 28, n. 3, 1994, 567-582.